Table A3. HMX freeze concentration data.
Run #1
Run #2
Run #3
Run #4
Run #5
Run #6
Temperature, ∞C
24.1
24.1
15
10
20
15
Freezing rate, mm/hr
11.7
6.7
3.8
2.1
9.4
5.4
Length of ice
cylinder, cm
HMX concentration, mg/L
2
0.77
1.19
1.02
0.31
0.81
0.30
4
0.73
0.53
0.23
0.04
0.57
0.18
6
0.79
0.35
0.11
0.01
0.63
0.12
8
0.89
0.41
0.06
0.01
0.73
0.15
10
0.99
0.34
0.03
0.02
0.75
0.34
12
1.13
0.38
0.04
0.03
0.88
0.24
14
1.21
0.46
0.08
0.05
1.05
0.27
16
1.26
0.47
0.07
0.05
1.36
0.47
18
1.46
0.62
0.12
0.07
1.59
0.68
20
0.63
0.21
0.46
2.23
1.04
22
0.81
0.33
1.02
24
0.57
26
Mean
1.02
0.56
0.24
0.10
1.06
0.44
Adj. mean*
1.00
0.47
0.13
0.03
0.95
0.39
†
% Removal
34.6
69.5
91.7
97.8
38.2
74.7
K
0.48
0.16
0.03
0.01
0.35
0.10
Residual
2.10
2.97
4.72
3.95
2.71
3.85
*Eliminate the first and last segments.
†
Concentration basis
Table A4. TNB freeze concentration data.
Run #1
Run #2
Run #3
Run #4
Run #5
Run #6
Temperature, ∞C
24.1
24.1
15
10
20
15
Freezing rate, mm/hr
11.7
6.7
3.8
2.1
9.4
5.4
Length of ice
cylinder, cm
TNB concentration, mg/L
2
0.87
1.39
1.23
0.36
0.90
0.35
4
0.75
0.60
0.24
0.05
0.61
0.22
6
0.81
0.37
0.12
0.01
0.68
0.15
8
0.98
0.48
0.05
0.01
0.81
0.20
10
1.12
0.39
0.03
0.02
0.85
0.37
12
1.35
0.44
0.03
0.02
1.01
0.32
14
1.46
0.52
0.06
0.05
1.21
0.37
16
1.65
0.53
0.06
0.04
1.40
0.57
18
1.87
0.66
0.11
0.07
1.61
0.78
20
0.70
0.24
0.72
2.25
1.11
22
0.87
0.37
1.22
24
0.64
26
Mean
1.21
0.63
0.27
0.14
1.13
0.51
Adj. mean*
1.16
0.52
0.13
0.03
1.02
0.45
†
% Removal
37.9
72.1
92.9
98.2
45.4
75.7
K
0.50
0.14
0.03
0.01
0.27
0.09
Residual
2.34
3.72
4.80
4.65
3.73
4.88
*Eliminate the first and last segments.
†
Concentration basis
10
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